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  3. 卓上型核磁気共鳴装置(卓上型NMR)
  4. スペクトル例 – 卓上型核磁気共鳴装置(卓上型NMR)

スペクトル例 – 卓上型核磁気共鳴装置(卓上型NMR)

卓上型核磁気共鳴装置(卓上型NMR)

X-Pulse

イギリス:オックスフォード・インストゥルメンツ社

1次元スペクトル

01_1H FID, 5-Bromo-1,2,3-trifluorobenzene in CDCl3
02_1H FID, Ethyl crotonate in CDCl3
03_1H-FID-Gemfibrozil-in-CDCl3
04_1H-FID-Ibuprofen-in-CD32SO
05_1H-CPMG-T2-Dimethyl-Carbonate
06_1H FID, 1,1,3,3,5,5-hexamethyltrisiloxane in C6D6
07_1H FID, 1,4-difluoro-2,5-dimethoxybenzene in CDCl3
08_1H FID, 1-Bromo-2,4,5-trifluorobenzene in CDCl3
09_1H-FID-methyl-3-methyl-2-butenoate-in-CDCl3
10_1H FID, Quinine in DMSO-d6
11_1H InvRec (T1), Dimethyl Carbonate
12_1H J-PGSE, Dimethyl Carbonate
13_1H PGSE, Dimethyl Carbonate
14_1H{13C} FID, DMC-DEC-EC
15_1H{31P} FID, OP(OMe)2Ph & dppe
16_1H FID, Acetylferrocene in CDCl3

13C

17_13C{1H} DEPT, Ethyl crotonate in CDCl3
18_13C{1H} DEPT, Ibuprofen in (CD3)2SO
19_13C{1H} DEPT, methyl 3-methyl-2-butenoate in CDCl3
20_13C{1H} DEPT, Quinine in DMSO-d6
21_13C{1H} FID, Ethyl Crotonate in CDCl3
22_13C{1H} FID, Gemfibrozil in CDCl3
23_13C{1H} FID, Ibuprofen in (CD3)2SO
24_13C{1H} FID, methyl 3-methyl-2-butenoate in CDCl3
25_13C{1H} FID, Quinine in DMSO-d6

11B

26_11B FID, [nBu4N][B(C6F5)4] in CD3CN
27_11B FID, Na[BF4] in D2O
28_11B{19F} FID, Na[BF4] in D2O

59Co

29_59Co FID, [Co(en)3]Cl3 in D2O
30_59Co FID, K3[Co(CN)6] in D2O

19F

31_19F FID, [nBu4N][B(C6F5)4] in CD3CN
32_19F FID, 1,4-difluoro-2,5-dimethoxybenzene in CDCl3
33_19F FID, 1-Bromo-2,4,5-trifluorobenzene in CDCl3
34_19F FID, 5-Bromo-1,2,3-trifluorobenzene in CDCl3
35_19F FID, Li[PF6] in DMC
36_19F FID, Na[BF4] in D2O
37_19F{11B} FID, Na[BF4] in D2O

23Na

38_23Na_FID, Na[BF4] in D2O

29Si

39_29Si{1H} DEPT-24, 1,1,3,3,5,5-hexamethyltrisiloxane in C6D6
40_29Si{1H} DEPT-90, 1,1,3,3,5,5-hexamethyltrisiloxane in C6D6

31P

41_31P FID, Li[PF6] in DMC
42_31P{1H} FID, OP(OMe)2Ph & dppe in CDCl3

27Al

43_27Al FID, Al(NO3)3 9H2O in D2O

7Li

44_7Li PGSE, Li[PF6] in PC

2次元スペクトル

1H-13C

45_1H-13C gs-HMBC, ethyl crotonate in CDCl3
46_1H-13C gs-HMBC, Gemfibrozil in CDCl3
47_1H-13C gs-HMBC, Ibuprofen in (CD3)2SO
48_1H-13C gs-HMBC, Quinine in DMSO-d6
49_1H-13C gs-HSQC-ME, ethyl crotonate in CDCl3
50_1H-13C gs-HSQC-ME, Gemfibrozil in CDCl3
51_1H-13C gs-HSQC-ME, Ibuprofen in (CD3)2SO
52_1H-13C HMBC, methyl 3-methyl-2-butenoate in CDCl3

1H-19F

53_1H-19F gs-COSY, 1,4-difluoro-2,5-dimethoxybenzene in CDCl3

1H-1H

54_1H-1H gs-COSY, ethyl crotonate in CDCl3
55_1H-1H gs-COSY, methyl 3-methyl-2-butenoate in CDCl3
56_1H-1H gs-NOESY, methyl 3-methyl-2-butenoate in CDCl3
57_1H-1H gs-TOCSY, ethyl crotonate in CDCl3
58_1H-1H gs-TOCSY, Ibuprofen in (CD3)2SO
59_1H-1H gs-TOCSY, methyl 3-methyl-2-butenoate in CDCl3

13C-1H

60_13C-1H HETCOR, Ibuprofen in (CD3)2SO

1H-29Si

61_1H-29Si gs-HMBC, 1,1,3,3,5,5-hexamethyltrisiloxane in C6D6

1H-29Si

62_31P-1H gs-HSQC, OP(OMe)2Ph & dppe in CDCl3

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卓上型核磁気共鳴装置 X-Pulse
イギリスオックスフォード・インストゥルメンツ社製
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